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약재백과 상세보기

홈 한약재기본검색약재백과 상세보기

치자, 梔子,Gardeniae Fructus

이화학

최종수정일 2023-11-21

참고문헌 스크랩 스크랩새창열기

주요성분 - Name, PubChemID, reference
Name PubChemID reference Name PubChemID reference
3,4-Di-O-caffeoylquinic acid 5281780 36 3,4-dicaffeoyl-5-(3-hydroxy-3-methylglutaroyl) quinic acid 없음 27
3,4-dicaffeoyl-5-(3-hydroxy-3-methylglutaroyl) quinic acid 없음 36 3,5-di-O-caffeoylquinic acid 6474310 36
4,5-di-O-caffeoylquinic acid 6474309 36 4-sinapoyl-5-caffeoylquinic acid 없음 36
5-O-caffeoylquinic acid 5315832 36 6"-O-trans-cinnamoylgenipin gentiobioside 없음 36
6"-O-trans-feruloylgenipin gentiobioside 없음 36 acetylgeniposide 없음 27
caffeoyl sinapoylquinic acid 6450024 27 chlorogenic acid 1794427 21
chlorogenic acid 1794427 28 chlorogenic acid 1794427 32
chlorogenic acid 1794427 37 chlorogenic acid 1794427 39
chlorogenic acid 1794427 46 chlorogenic acid 1794427 49
croceic acid 5281232 46 crocetin 5281232 27
crocetin 5281232 37 crocin 1 5281233 27
crocin 1 5281233 37 crocin 2 9940690 27
crocin 2 9940690 37 crocin 3 10461942 27
crocin 3 10461942 37 crocin I 5281233 32
crocin II 9940690 32 crocin-1 5281233 21
crocin-1 5281233 28 crocin-1 5281233 39
crocin-1 5281233 42 crocin-1 5281233 46
crocin-2 9940690 21 crocin-2 9940690 28
crocin-2 9940690 42 crocin-2 9940690 46
crocin-3 10461942 42 crocin-I 5281233 36
deacetyl-asperulosidic acid 12315350 36 deacetyl-asperulosidic acid methyl ester 6325021 36
gardenoside 442423 27 gardenoside 442423 36
gardenoside 442423 37 gardenoside 442423 46
gardenoside 442423 49 gardoside 46173850 36
genepin-1-β-D-gentiobioside 3082301 37 genipin 442424 21
genipin 442424 32 genipin gentobioside 3082301 27
genipin-1-β-D-gentiobioside 3082301 36 genipin-1-β-genitiobioside 3082301 46
genipin-1-β-gentiobioside 3082301 21 genipin-1-β-gentiobioside 3082301 28
geniposic acid 443354 49 geniposide 107848 21
geniposide 107848 27 geniposide 107848 28
geniposide 107848 32 geniposide 107848 36
geniposide 107848 37 geniposide 107848 39
geniposide 107848 42 geniposide 107848 45
geniposide 107848 46 geniposide 107848 49
geniposidic acid 443354 21 geniposidic acid 443354 28
geniposidic acid 443354 32 geniposidic acid 443354 36
geniposidic acid 443354 46 quercetin-3-O-rutinoside 5280805 36
quercetin-3-rutinoside 5280805 27 rutin 5280805 21
rutin 5280805 28 rutin 5280805 37
rutin 5280805 39 scandoside methyl ester 442433 27
scandoside methyl ester 442433 36 scandoside methyl ester 442433 46
shanzhiside 11948668 36 shanzhiside methyl ester 1794427 32

열기 접기

HPLC

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
1 g water 50 mL boiling 5, 15 min, 2 batches 45

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Bioanalytical System BAS PM-80 pump (IN, USA) with a Rheodyne 9125 injector (CA, USA) equipped with a 20 μl sample loop, and a Varian Dynamax UV–Vis detector (CA, USA)
Column Nova-Pak reversed-phase column (RP-C , 150 × 3.9 mm, 4 μm, Waters, Milford, MA)
Detector Varian Dynamax UV–Vis detector
Wave 240 nm
Phase acetonitrile-methanol-5 mM monosodium phosphate (pH 4.6) (5:15:80) (v/v/v) (A)
Density 없음
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/12186394

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
0.1 g 50% methanol 30 mL RT, ultrasonication 30 min 39

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Agilent 1200 (Agilent Technologies, Palo Alto, CA, USA) with diode array detector
Column Agilent Zorbax Extend C18 (250 mm × 4.6 mm, 5 μm), 25°C
Detector diode array detector
Wave 240 nm, 254 nm, 330 nm, 440 nm
Phase aqueous phosphoric acid (0.4%,v/v) (A) and acetonitrile (B)
Density 20μl
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/22262927

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
1 g 50% methanol 3 ×10 mL utrasonication 40 min 27

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System HPLC system consisted of a HP 1100L instrument equipped with a HP 1040 diode-array detector (DAD) with a HP 1100 MSD API-electrospray (Agilent Technologies, Palo Alto, CA, USA)
Column Phenomenex Luna C18 (250 × 4.6 mm, 5 μm), 27°C
Detector diode-array detector
Wave 240 nm. 315nm, 438nm
Phase methanol (A) and water (pH 3.2, HCOOH) (B)
Density 20μl
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/23107748

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
0.1 g 50% methanol 50 mL utrasonication 30 min 21

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Agilent 1200 HPLC system with diode array detector and a LC/MSD Trap XCT electrospray ion mass spectrometer (Agilent Corporation, USA)
Column Agilent ZORBAX SB-C18 analytical column (1.8 μm, 2.1 mm × 50 mm, i.d.) wi
Detector LC/MSD Trap XCT electrospray ion mass spectrometer
Wave negative ion mode, capillary potential 3.5 kV, cone voltage 110 V, electrospray source temperature 135 °C, desolvation temperature 400 °C, nitrogen nebulizing gas flow 50 l/h, nitrogen desolvation gas flow 350 l/h, fragmentation energy at 110 V
Phase water with 0.1% formic acid (A) and acetonitrile (B)
Density 2μl
Flow 0.2 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/24183952

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
1.0 g 70% methanol 200 mL ultrasonication 60 min 49

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Waters 600 HPLC system (Waters, USA)
Column AKZO NOBEL Kromasil 100-5C18 column (5 μm, 250 × 4.6 mm), 25°C
Detector diode-array detector
Wave 없음
Phase water with 1 % acetic acid (A) and acetonitrile with 1 % acetic acid (B)
Density 20μl
Flow 0.6 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/24277694

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
100 g 50% ethanol 800 mL reflux 1 hr 36

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Varian ProStar HPLC system (Agilent Technologies, USA) consisted of a ProStar 210 pump, a 410 analytical type auto-sampler, a 330 photodiode-array UV detector (PDA) and Star workstation
Column Unitary C18 column (4.6 mm × 250 mm, 5 μm), 25°C
Detector photodiode array detector
Wave 238 nm
Phase water–formic acid (100:0.1, v/v) (A) and acetonitrile (B)
Density 20μl
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/26041243

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
100 g 50% ethanol 800 mL reflux 1 hr 36

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Ultimate 3000 liquid chromatograph system equipped with a diode array detector and a thermo LCQ FLEET (Thermo Finnigan, San Jose, CA, USA) mass spectrometer via an ESI interface
Column Unitary C18 column (4.6 mm × 250 mm, 5 μm), 25°C
Detector ESI-MS
Wave positive and negative ion mode, full mass (m/z 100–1000), MS2 of the most abundant ion in the full mass and MS3 of the most abundant ion in the MS2, Electrospray voltage 4 kV, capillary temperature 350℃ capillary voltage ±35 V, lens voltage ±75 V, sheath gas pressure 35 psi, auxiliary gas flow rate 8 arb (1 arb = 0.3 l/min), normalized energy of collision 35%, the post-column split ratio 7:3
Phase water–formic acid (100:0.1, v/v) (A) and acetonitrile (B)
Density 20μl
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/26041243

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
0.5 g methanol 25 mL ultrasonication 30 min 46

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Agilent series 1100 HPLC system equipped with a quaternary pump, a variable wavelength detector (VWD), a manual injector, and a column compartment
Column Akzo Nobel Kromasil 100-5C18 column (250 mm × 4.6 mm i.d., 5 μm), 25°C
Detector variable wavelength detector (VWD)
Wave 238 nm
Phase methanol (A) and 0.4% (v/v) acetate acid in water (B)
Density 10μl
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://search.proquest.com/docview/1282134075?pq-origsite=gscholar

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
1.0 g 75% methanol 20 mL ultrasonication 30 min 32

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Acquity UPLC-PDA, consisting of a vacuum degasser, binary solvent delivery pump, autosampler, and thermostated column compartment (Waters, Milford, MA, USA)
Column Waters Acquity BEH C18 column (50 × 2.1 mm, 1.7 μm), 35°C
Detector photodiode array detector
Wave 200 nm, 480 nm
Phase acetonitrile (A) and 0.2% formic acid water (B)
Density 2μl
Flow 0.6 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL http://www.academicjournals.org/article/article1380716789_Yang%20et%20al.pdf

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
0.4 g 50% methanol 50 mL ultrasonication 30 min 28

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Waters 2695 HPLC system (Waters, USA) with 2998 photodiode array detector
Column SinoChrom ODS-BP C18 column (4.6 × 250 mm, 5 μm) (Elite Analytical Instruments Co., Ltd, China), 30°C
Detector photodiode array detector
Wave 254 nm
Phase water with 0.1% formic acid (A) and acetonitrile (B)
Density 5μl
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/26071608

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
0.1 g 50% ethanol 50 mL ultrasonication 30 min 42

HPLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
System Shimadzu HPLC system equipped with two LC-10AT VP pumps, CTO-10AS VP column oven, UV–Vis SPD-10A VP detector
Column ODS column (150× 4 mm, Shimadzu, Japan)
Detector shimadzu UV–Vis SPD-10A VP detector
Wave 238 nm (0-20 min), 440 nm (20-60 min)
Phase water (A) and acetonitrile (B)
Density 없음
Flow 1 ml/min
이동상
시간 (분) 이동상 (%)
해당자료 없음.
URL https://www.ncbi.nlm.nih.gov/pubmed/19815056

TLC

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
없음 없음 없음 없음 없음 37

TLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
Method 200 mg을 10 mL을 methanol:water (50:50, v/v)을 사용하여 40분, 20°C 초음파 추출
Absorbent 박층크로마토그래프용실리카겔 (LiChrospher HPTLC Silica gel 60 RP-18 W F254, 20 cm × 10 cm plates)
Solvent acetonitrile : 0.1% formic acid (40 : 60 v/v)
Wave UV 254 nm (A), 366 nm (B), white light ©
Indentification HPTLC fingerprint of Gardenia Jasminoides Ellis fruits (B3 extract) at 254 nm (A), 366 nm (B) and white light (C), together with their densitograms at 240, 330 and 440 nm, respectively. 1 gardenoside, 2 genepin-1-β-D-gentiobioside, 3 geniposide, 4 crocin 1, 5 crocin 2, 6 crocin 3, 7 crocetin, 8 dicaffeoylquinic acid, 9 sinapoylquinic acid.
Compound gardenoside, genepin-1-β-D-gentiobioside, geniposide, crocin 1, crocin 2, crocin 3, crocetin, dicaffeoylquinic acid, sinapoylquinic acid
URL https://www.ncbi.nlm.nih.gov/pubmed/24365117

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
없음 없음 없음 없음 없음 37

TLC - System, Column, Detector, Wave, Phase, Density, Flow, URL
Method 200 mg을 10 mL을 methanol:water (50:50, v/v)을 사용하여 40분, 20°C 초음파 추출
Absorbent 박층크로마토그래프용실리카겔 (LiChrospher HPTLC Silica gel 60 RP-18 W F254, 20 cm × 10 cm plates)
Solvent acetonitrile : 0.1% formic acid (40 : 60 v/v)
Wave diphenylborinic acid aminoethylester in ethyl acetate (NP) reagent, UV 365 nm (A), 2,2-diphenyl-1-picrylhydrazyl (DPPH) reagent, white light (B), vanillin-sulfuric acid reagent (VS) reagent, white light ©
Indentification Derivatized HPTLC finger prints of Gardenia Jasminoides Ellis fruits (B3 extract). A: NP reagent, UV 366 nm; B: DPPH reagent, white light; C: VS reagent, white light. 1 gardenoside, 2 genepin-1-β-D-gentiobioside, 3 geniposide, 8 dicaffeoylquinic acid, 9 sinapoylquinic acid, 10 rutin, 11 chlorogenic acid.
Compound gardenoside, genepin-1-β-D-gentiobioside, geniposide, dicaffeoylquinic acid, sinapoylquinic acid, rutin, chlorogenic acid
URL https://www.ncbi.nlm.nih.gov/pubmed/24365117

기타

추출물정보

추출물정보 (성분명1) - 시료무게, 용매, 용매용량, 온도, 시간, 참고문헌
시료무게 용매 용매용량 온도 시간 참고문헌
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